[1]陶厚璜,周泓彬,郭明.凝脂莲香精成分分析及最优提取方式研究[J].浙江林业科技,2024,44(01):25-32.[doi:10.3969/j.issn.1001-3776.2024.01.004]
 TAO Houhuang,ZHOU Hongbin,GUO Ming.The Optimal Technology for Extraction of Essential Oil and Analysis on Its Components from Sedum clavatum[J].Journal of Zhejiang Forestry Science and Technology,2024,44(01):25-32.[doi:10.3969/j.issn.1001-3776.2024.01.004]
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凝脂莲香精成分分析及最优提取方式研究()
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《浙江林业科技》[ISSN:1001-3776/CN:33-1112/S]

卷:
44
期数:
2024年01期
页码:
25-32
栏目:
研究报告
出版日期:
2024-01-20

文章信息/Info

Title:
The Optimal Technology for Extraction of Essential Oil and Analysis on Its Components from Sedum clavatum
文章编号:
1001-3776(2024)01-0025-08
作者:
陶厚璜周泓彬郭明
(浙江农林大学 化学与材料工程学院,浙江 杭州 311300)
Author(s):
TAO HouhuangZHOU HongbinGUO Ming
(College of Chemistry and Materials Engineering, Zhejiang A & F University, Hangzhou 311300, China)
关键词:
凝脂莲微波辅助水蒸气法香精气相色谱-质谱联用单因素实验正交试验
Keywords:
Sedum clavatum microwave assisted hydro distillation essential oil gas chromatography-mass spectrometry single factor experiment orthogonal test
分类号:
S682.33;Q946
DOI:
10.3969/j.issn.1001-3776.2024.01.004
文献标志码:
A
摘要:
提取景天科Crassulaceae 植物凝脂莲Sedum clavatum 的香精成分,并分析不同部位香精组分差异性,提 高凝脂莲香精提取的产量。采用微波辅助水蒸气法提取植株、叶片以及茎秆部位的香精,气相色谱-质谱联用 技术分析凝脂莲植株、叶片与茎秆香精的成分,通过单因素实验探求香精提取的最佳条件,正交实验筛选最优 条件组合。研究发现茎秆部位提取率大约为叶片部位提取率的4 倍,茎秆香精与植株香精成分重复物质为2 种, 占植株香精成分的16.91%。实验结果表明,在固液比1∶8、浸泡时间60 min、微波功率400 W、提取时间3 h 的条件下,提取率最高,最高提取率为0.96%。
Abstract:
Extraction of essential oil from the whole plant, leaves and stem of Sedum clavatum was implemented by microwave assisted hydro-distillation, and analysis were made on their component by gas chromatography-mass spectrometry. The optimal technology for extraction was experimented with single factor and orthogonal design. The result demonstrated that the extraction rate of essential oil from stem was about 4 times higher than that from leaf, and there were 2 same substances in essential oil from stem and the whole plant. The experiment showed the optimal technology for extraction of essential oil from different part of S. clavatum was as follows: solid-liquid ratio of 1:8, soaking time of 60 min, microwave power of 400 W, and extraction time of 3 h, the highest extraction rate reached 0.96%.

参考文献/References:

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备注/Memo

备注/Memo:
收稿日期:2023-03-20;修回日期:2023-12-02
基金项目:浙江省公益基金项目资助(LGN20B070001)
作者简介:陶厚璜,硕士研究生,从事林源天然产物分析研究;E-mail: 1918763910@qq.com。通信作者:郭明,教授,从事天然产物研究; E-mail: guoming@zafu.edu.cn。
更新日期/Last Update: 2024-02-20