[1]张辉,林秀君,陈莉娟,等.响应面试验优化日本冷杉针叶精油提取工艺[J].浙江林业科技,2023,43(02):41-46.[doi:10.3969/j.issn.1001-3776.2023.02.007]
　ZHANG Hui,LIN Xiu-jun,CHEN Li-juan,et al.Optimization for Extraction of Essential Oil from Needles of Abies firma by ResponseSurface Methodology[J].Journal of Zhejiang Forestry Science and Technology,2023,43(02):41-46.[doi:10.3969/j.issn.1001-3776.2023.02.007]
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响应面试验优化日本冷杉针叶精油提取工艺()
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《浙江林业科技》[ISSN:1001-3776/CN:33-1112/S]

卷:
43
期数:
2023年02期
页码:
41-46
栏目:
出版日期:
2023-03-20

文章信息/Info

Title:
Optimization for Extraction of Essential Oil from Needles of Abies firma by ResponseSurface Methodology
文章编号:
1001-3776（2023）02-0041-06
作者:
张辉 1; 林秀君1; 陈莉娟1; 刘浩凯2; 严邦祥1; 赵昌高1; 李桥2
(1. 景宁畲族自治县生态林业发展中心，浙江景宁 323500；2. 景宁县畲族自治县自然资源和规划局，浙江景宁 323500)
Author(s):
ZHANG Hui1; LIN Xiu-jun1; CHEN Li-juan1; YAN Bang-xiang1; ZHAO Chang-gao1; LI Qiao2; LIU Kai-hao2
(1. Ecological Forestry Development Center of She Autonomous County of Zhejiang, Jingning 323500, China2. Natural Resources and Planning Bureau of She Autonomous County of Zhejiang, Jingning 3235000, China)
关键词:
日本冷杉; 精油; 提取工艺; 响应面试验
Keywords:
Abies firma;  essential oil;  extraction process;  response surface methodology (RSM)
分类号:
S791.149；O658.3
DOI:
10.3969/j.issn.1001-3776.2023.02.007
文献标志码:
A
摘要:
利用响应面（RSM）分析优化日本冷杉Abies firma 针叶精油的提取工艺。以日本冷杉精油得率为考察指标，在样品粉碎粒度、浸泡时间、蒸馏时间、蒸馏速度4 个单因素实验基础上，通过响应面法的Box-Behnken 实验设计对日本冷杉针叶精油水蒸气蒸馏法提取工艺进行优化，建立二次多项式回归方程的预测模型。日本冷杉针叶精油的优化提取工艺为：粉碎粒度200 目、浸泡时间37 min、蒸馏时间108 min、蒸馏速度2.8 mL·min-1。在此优化条件下的精油最大得率为0.714%，与预测值0.716%具有很好的一致性，表明采用响应面优化得到的日本冷杉精油提取工艺条件可靠，可为日本冷杉针叶中精油的提取方法提供参考。
Abstract:
In September 2020, needles of introduced 20-year Abies firma were collected from Jinning Caoyutang Forest Park, Zhejiang province.Essential oil from needles were prepared by steam distillation with water as solvent, and response surface methodology (RSM) was used to optimizethe extraction process. Taking the yield of essential oil as objective, four single factors were tested like particle size, soaking time, distillation timeand distillation speed. The extraction process of A. firma essential oil by steam distillation was optimized through Box Behnken design of responsesurface methodology, and a prediction model of quadratic polynomial regression equation was established. The optimal extraction process of theessential oil from A. firma needles was as follows: 200 mesh of particle size, 37 minutes of soaking, 108 minutes of distillation, and 2.8 mL/min ofthe distillation speed. Under this condition, the maximum yield of essential oil was 0.714%, which was in good conformity with the predicted value of0.716%, indicating that the extraction process was reliable.

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备注/Memo

备注/Memo:
收稿日期：2022-10-04；修回日期：2023-02-06
基金项目：景宁畲族自治县科技计划项目（2020A5）；景宁科技计划项目（2022A8）
作者简介：张辉，硕士研究生，林业工程师，从事森林资源保护培育与开发利用研究；E-mail:taoyuan31@126.com。通信作者：林秀君，工程师，从事林业技术推广、森林资源保护研究；E-mail:jnlxj2021@163.com。
更新日期/Last Update: 2023-03-20